Journal of Organometallic Chemistry p. 411 - 434 (1985)
Update date:2022-08-03
Topics:
Brauer, David J.
Hietkamp, Sibbele
Sommer, Herbert
Stelzer, Othmar
Mueller, Gerhard
et al.
The triphosphaalkane Cl2PCH2PClCH2PCl2 (III) is formed as a by-product in the synthesis of Cl2PCH2PCl2 (II).On treating III with MeMgCl or EtOH (in the presence of a base), the methyl or ethoxy derivative (V or VI) may be obtained in satisfactory yields.With Ni(CO)4 or Fe2(CO)9 V forms trinuclear complexes <(CO)nM>PMe2CH2PMe
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