Canadian Journal of Chemistry p. 554 - 557 (1982)
Update date:2022-07-29
Topics:
Robins, Morris, J.
Barr, Philip J.
Giziewicz, Jerzy
Treatment of uracil bases and protected nucleosides with iodine monochloride (ICl) gave the corresponding 5-iodouracil products in over 95percent purified yields.Analogously facile chlorination was effected with iodobenzene dichloride (PhICl2).Protection of the nucleosides as p-toluyl esters provided reactants that were soluble in organic solvents and crystallized readily in high yields.
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(1981)Doi:10.1016/S0040-4039(00)86853-7
(1982)Doi:10.1016/S0040-4039(00)86984-1
(1982)Doi:10.1016/S0040-4039(00)87003-3
(1982)Doi:10.1016/0008-6215(93)80100-S
(1993)Doi:10.1021/jo00139a018
(1982)