Synthetic Communications p. 659 - 663 (2006)
Update date:2022-08-02
Topics: Deprotection Protection Acetals MoO3/SiO2
Bhosale, Rajesh S.
Bhosale, Sidhanath V.
Bhosale, Sheshanath V.
Solanke, Kuldeep S.
Pawar, Rajendra P.
Chougule, Harish S.
Dongare, Mohan K.
Acetalization of aldehydes using a new silica-supported molybdenum(VI) oxide (20%) catalyst has been explored. Additionally, facile deprotection strategy for the acetals is reported including the results from the replacement of solvent studies. The protocol achieved the protection O,O-acetals in excellent yield within a few hours under neutral conditions and also deprotection of aromatic O,O-acetals in excellent yields was achieved within a few minutes in aqueous acetone. Copyright Taylor & Francis Group, LLC.
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