Chemistry Letters p. 921 - 924 (1982)
Update date:2022-07-30
Topics:
Matsueda, Rei
Higashida, Susumu
Ridge, Richard J.
Matsueda, Gary R.
All the conventional S-protecting groups of cysteine which were tested could be selectively converted to the 3-nitro-2-pyridine-sulfenyl (Npys) group after treatment with an appropriate Npys halide.Unidirectional formation of an unsymmetrical disulfide bond is possible when Cys(Npys) is mixed with a free thiol of another Cys residue.Some of these features were exploited during the solid phase synthesis of lysine8-vasopressin.
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