Journal of the Chemical Society. Chemical communications p. 1407 - 1408 (1995)
Update date:2022-08-03
Topics:
Ogawa, Takuji
Yoshikawa, Akemi
Wada, Hidemi
Ogawa, Chie
Ono, Noboru
Suzuki, Hitomi
Tris(2-methoxyphenyl)bismuthane works as both a mild dehydrating agent and a good template for macrocyclic ester synthesis; prolonged heating of the bismuthane with a dicarboxylic acid anhydride and a glycol in toluene under reflux afforded the corresponding macrocyclic 1:1 diester in moderate to good yields, together with a small amount of a macrocyclic 2:2 tetraester.
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Doi:10.1016/S0040-4039(01)90166-2
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