Highly Substituted Dienes from Butyne-1,4-diol. A One-flask Synthesis and the Mechanism of Formation of 3-(N,N-Diethylamino)-2-phenylsulphinylbutadiene

DOI: 10.1039/c39820000665

Source and publish data:

Journal of the Chemical Society. Chemical communications p. 665 - 666 (1982)

Update date:2022-08-05

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Authors:

Bridges, Alexander J.

Fischer, John W.

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Article abstract of DOI:10.1039/c39820000665

When 4-acetoxybut-2-yn-1-ol is treated with benzenesulphenyl chloride and triethylamine, followed by diethylamine, 3-(N,N-diethylamino)-2-phenylsulphinylbutadiene is produced, in a multistep process, in 90percent overall yield.

Full text of DOI:10.1039/c39820000665

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