Tetrahedron Letters p. 4649 - 4652 (1999)
Update date:2022-08-04
Topics:
Wipf, Peter
Reeves, Jonathan T.
A recyclable fluorous labeled THP protecting group has been developed that allows for simple purification of small molecules by liquid-liquid extraction with FC-72/MeCN, and of larger or more polar molecules by solid phase extraction with fluorous reverse phase silica gel. In addition, we report a new glycosylation method which uses the Cp2ZrCl2-AgClO4 reagent system to activate an anomeric sulfoxide.
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