Synthesis and applications of a fluorous THP protective group

DOI: 10.1016/S0040-4039(99)00866-7

Source and publish data:

Tetrahedron Letters p. 4649 - 4652 (1999)

Update date:2022-08-04

Topics:

Authors:

Wipf, Peter

Reeves, Jonathan T.

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Article abstract of DOI:10.1016/S0040-4039(99)00866-7

A recyclable fluorous labeled THP protecting group has been developed that allows for simple purification of small molecules by liquid-liquid extraction with FC-72/MeCN, and of larger or more polar molecules by solid phase extraction with fluorous reverse phase silica gel. In addition, we report a new glycosylation method which uses the Cp₂ZrCl₂-AgClO₄ reagent system to activate an anomeric sulfoxide.

Full text of DOI:10.1016/S0040-4039(99)00866-7

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