A TOTAL SYNTHESIS OF 6"-EPIVALIDAMYCIN A AND ITS DIASTEREOMER

DOI: 10.1246/cl.1983.1085

Source and publish data:

Chemistry Letters p. 1085 - 1088 (1983)

Update date:2022-08-03

Topics:

Authors:

Ogawa, Seiichiro

Inoue, Makoto

Iwasawa, Yoshikazu

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Article abstract of DOI:10.1246/cl.1983.1085

A total synthesis of the 6"-epimer of validamycin A and its diastereomer has been accomplished by a coupling reaction of the racemic peracyl 5,6-dihydroxy-1-hydroxymethyl-1,3-cyclohexadiene monoepoxide, the precursor of the unsaturated branched-chain cyclitol portion, with the protected β-D-glucopyranosylvalidamine, followed by acid hydrolysis and O-deacylation.

Full text of DOI:10.1246/cl.1983.1085

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