Synthesis of 2-exo-Hydroxy-4-thiahomoadamantane and Some Related Derivatives

DOI: 10.1021/jo00170a039

Source and publish data:

Journal of Organic Chemistry p. 4073 - 4076 (1983)

Update date:2022-08-05

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Authors:

Sasaki, Tadashi

Eguchi, Shoji

Ban, Hiroshi

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Article abstract of DOI:10.1021/jo00170a039

Treatment of 3-endo<(tosyloxy)methyl>-6,7-epoxybicyclo<3.3.1>nonane (2) with sodium sulfide gave 2-exo-hydroxy-4-thiahomoadamantane (4) in good yields.PCC oxidation of 4 afforded the corresponding ketone 9 and 3-thiatricyclo<5.3.1.0^4,9>undec-5-

Full text of DOI:10.1021/jo00170a039

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