Chemistry Letters p. 1121 - 1124 (1983)
Update date:2022-08-03
Topics:
Aoki, Mario
Uyehara, Tadao
Kato, Tadahiro
Kabuto, Kuninobu
Yamaguchi, Shozo
Cis and trans 1-hydroxy-neocembrenes were prepared in an enantiomerically pure form by reduction of dl-ketone with respective (+)- and (-)-Darvon-LiAlH4 complex followed by purification with the aids of esterification with d- and l-menthoxyacetyl chlorides and (-)-camphanic acid chloride, respectively.Absolute configuration of naturally occurring (+)-mayol and (+)-cembrenene was determined by correlation with enantiomerically pure compounds.
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