SYNTHESIS OF HEXAKIS(ARYLOXY)BENZENES : X-RAY ANALYSIS OF HEXAKIS(PHENYLOXY)BENZENE AND OF THE ACETONITRILE CLATHRATE OF HEXAKIS(3,5-DIMETHYLPHENYLOXY)BENZENE

DOI: 10.1016/S0040-4039(00)88154-X

Source and publish data:

Tetrahedron Letters p. 3269 - 3272 (1983)

Update date:2022-08-03

Topics:

Authors:

Gilmore, Christopher J.

MacNicol, David D.

Murphy, Anthony

Russell, Marie A.

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Article abstract of DOI:10.1016/S0040-4039(00)88154-X

Hexakis(aryloxy)benzenes (I)-(IV), representatives of a new class of molecule, have been prepared by reaction of hexafluorobenzene with the sodium salt of the appropriate phenol in 1,3-dimethyl-2-imidazolidinone (DMEU) as solvent.X-ray analyses of parent (I) and of the acetonitrile clathrate of (II) are described, a novel edge-on interaction between host and guest being found in the latter.

Full text of DOI:10.1016/S0040-4039(00)88154-X

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