Synlett p. 983 - 985 (2007)
Update date:2022-07-29
Topics:
Doan, Huynh Dong
Gallon, Julien
Piou, Alexandre
Vatèle, Jean-Michel
A short approach to the tetrahydrofuran fragment of amphidinolides X and Y has been developed through the combination of iterative Sharpless asymmetric epoxidations, Pd-catalyzed regioselective hydrogenolysis of a 4,5-epoxy-2-alkenoate and the disfavored 5-endo-tet ring closure of a β-hydroxy epoxide promoted by a double bond adjacent to the epoxide function. Georg Thieme Verlag Stuttgart.
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