Tetrahedron Letters p. 4303 - 4306 (1984)
Update date:2022-08-04
Topics:
Gilmore, Christopher J.
MacNicol, David D
Murphy, Anthony
Russel, Marie A.
In 1,3-dimethyl-2-imidazolidinone (DMEU) as solvent, pentafluoropyridine reacts with PhSNa to give an essentially quantitative yield of pentakis(phenylthio)pyridine (1); however, analogous reaction with pentachloropyridine leads to the unexpected co-formation of the title compound (2), a new host whose crystal structure has been elucidated by X-ray methods for both the unsolvated crystal and for the chlorobenzene inclusion compound.
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