Journal of Organic Chemistry p. 2622 - 2624 (1985)
Update date:2022-08-02
Topics:
Rathke, Michael W.
Cowan, Patrick J.
In the presence of magnesium chloride and 2 equiv of triethylamine, diethyl malonate is C-acylated in excellent yields by acid chlorides.A variety of other metal chlorides were ineffective.Similarly, ethyl acetoacetate is C-acylated by acid chlorides in the presence of magnesium chloride and 2 equiv of pyridine.
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