Monatshefte fur Chemie p. 645 - 650 (1985)
Update date:2022-08-05
Topics: Amine Yield NMR spectroscopy Catalyst Chromatography Recrystallization Mass spectrometry (MS) Aldehyde TLC (thin-layer chromatography) HPLC (high-performance liquid chromatography) Protecting group Anhydrous conditions Workup Reductive Amination N-Substitution Stoichiometry Inert atmosphere Solvent extraction pH adjustment
Angrick, Michael
O-Benzyl-N-(benzyloxycarbonyl)-DL-serine methyl ester (1a) and peptides 1b-d with C-terminal O-benzylserine ester have been reduced with diisobutylaluminium hydride to yield the N-substituted aminoglyceraldehydes 2a-d.Using lithium tetrahydridoaluminate as the reducing agent the corresponding alcohols 3a-d have been obtained. - (Keywords: Maillard reaction; N-Substituted aminoglyceraldehydes)
View MoreAnhui Sholon New Material Technology Co., Ltd.
website:http://www.sholonchem.com
Contact:+86-550-5261666
Address:4/F Block B, Beijing Chemical Building.No.520 Tianrun Road ,Science & Education Town Wujin District, Changzhou City Jiangsu Province
ZHIJIANG ZENVA SINO COMMERCE AND TRADE CO., LTD.
website:http://www.zenvasino.com
Contact:+86-138-72658998
Address:Shibeishan Road,Zhijiang, Hubei, China
Contact:+86-310-7092106
Address:Quzhou Modern & New Industrial Park, Handan, Hebei 057250, China
NINGBO PANGS CHEM INT’L CO., LTD.
Contact:+86-0574-27666801
Address:Floor 21, Building 11, Xintiandi, No. 689, Shijiroad, Ningbo, Zhejiang, China
WUHU HUAHAI BIOLOGY ENGINEERING CO LTD
Contact:+86-553-3836920
Address:7/F NO.82 LAODONG ROAD WUHU CHINA
Doi:10.1021/ja01352a051
(1931)Doi:10.1016/0022-328X(85)80037-1
(1985)Doi:10.1021/ja01547a025
(1958)Doi:10.1002/hlca.19510340117
(1951)Doi:10.1021/ja01546a023
(1958)Doi:10.1246/cl.1985.579
(1985)
