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Stereoselective S-Oxidation of 5-Substituted 4-Acetyl-Δ2-1,3,4-thiadiazolines: X-Ray Crystal Structure of 4-Acetyl-2-acetylamino-5-methyl-5-phenyl-Δ2-1,3,4-thiadiazoline 1-Oxide

DOI: 10.1039/c39820000901

Source and publish data:

Journal of the Chemical Society. Chemical communications p. 901 - 902 (1982)

Update date:2022-08-11

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Authors:

Kubota, SeijuKubota, Seiju

Toyooka, KouheiToyooka, Kouhei

Yamamoto, NaoyaYamamoto, Naoya

Shibuya, MasayukiShibuya, Masayuki

Kido, MasaruKido, Masaru

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Article abstract of DOI:10.1039/c39820000901

N.m.r. spectroscopy and X-ray crystallography show that oxidation of 5-substituted 4-acetyl-2-acetylamino-Δ2-1,3,4-thiadiazolines with m-chloroperbenzoic acid gives the corresponding Δ2-1,3,4-thiadiazoline 1-oxides; the novel reactions of the product (2a) are also described.

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