Nucleosides and Nucleotides p. 1223 - 1224 (1999)
Update date:2022-08-10
Topics:
Gunzenhauser
Biala
Strazewski
3,6,9-Trioxaundecane-1,11-diisocyanate (6) was synthesised from tetraethylene glycol in 5 steps and 48 % overall yield. Spacer 6 was monofunctionalised with the fully protected adenosyl-3'-O-succinate derivative 7 and linked to aminomethyl polystyrene affording a solid support suitable for oligoribonucleotide synthesis (loading: ~20 μmol/g). The HPLC analysis of a crude oligoribonucleotide synthesis and the yield of the full- length product show that this spacer compares well to hexamethylene diamine.
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