Chemistry Letters p. 309 - 312 (1984)
Update date:2022-08-30
Topics:
KIM, Yong Hae
YON, Gyu Hwan
KIM, Hyung Jin
Treatment of 1,3-disubstituted thioureas with superoxide radical anion (O2.-) at 20 deg C in dimethyl sulfoxide resulted in the formation of 1,3-disubstituted ureas in excellent yields.The desulfurization appears to proceed by the formation of peroxy-sulfur intermediates such as peroxy-sulfenate, -sulfinate and/or -sulfonate.
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