ELECTROCATALYZED CARBOXYLATION OF ORGANIC HALIDES BY COBALT-SALEN COMPLEX.

DOI: 10.1016/S0040-4039(00)98122-X

Source and publish data:

Tetrahedron Letters p. 2633 - 2636 (1985)

Update date:2022-08-11

Topics:

Authors:

Folest, Jean-Claude

Duprilot, Jean-Marc

Perichon, Jacques

Robin, Yvette

Devynck, Jacques

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Article abstract of DOI:10.1016/S0040-4039(00)98122-X

The carboxylation of benzylic and allylic chlorides by CO2 in tetrahydrofuran + hexamethylphosphoramide (40percent -60percent) is electrocatalyzed by cobalt Schiff-base complex Co(Salen).The reactions were performed by controlled-potential electrolysis at the R-Co(Salen) reduction potential.The yield of the carboxylic acid formation has been calculated.

Full text of DOI:10.1016/S0040-4039(00)98122-X

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