Tetrahedron Letters p. 2633 - 2636 (1985)
Update date:2022-08-11
Topics:
Folest, Jean-Claude
Duprilot, Jean-Marc
Perichon, Jacques
Robin, Yvette
Devynck, Jacques
The carboxylation of benzylic and allylic chlorides by CO2 in tetrahydrofuran + hexamethylphosphoramide (40percent -60percent) is electrocatalyzed by cobalt Schiff-base complex Co(Salen).The reactions were performed by controlled-potential electrolysis at the R-Co(Salen) reduction potential.The yield of the carboxylic acid formation has been calculated.
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