Bulletin of the Chemical Society of Japan p. 3659 - 3662 (1987)
Update date:2022-08-11
Topics:
Kanoh, Shigeyoshi
Muramoto, Hiroki
Kobayashi, Natsumi
Motoi, Masatoshi
Suda, Hiroshi
Racemic 6,6'-dimethylbiphenyl-2,2'-dicarboxylic acid (1) could be conveniently synthesized and efficiently resolved by the recrystallization of the brucine salts in satisfactory yields.Each enantiomer, thus obtained, was confirmed to be optically pure from a high-performance liquid chromatographic (HPLC) analysis on an optically active column.
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