Chemical Communications p. 1497 - 1498 (1996)
Update date:2022-08-16
Topics:
Kroecher, Oliver
Koeppel, Rene A.
Baiker, Alfons
Hybrid materials derived from group VIII metal-chloro complexes of the type MCl2X2 (M = Pt, Pd), MClX3 (M = Rh, Ir) and especially RuCl2X3 [X = Ph2P(CH2)2Si(OEt)3, Me2P(CH2)2Si(OEt)3] by cocondensation with Si(OEt)4 via a sol-gel process are highly active heterogeneous catalysts for the synthesis of N,N-dimethylformamide (dmf) from CO2, H2 and dimethylamine under supercritical conditions, affording turnover numbers up to 110 800 at 100% selectivity.
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