Tetrahedron Letters p. 3179 - 3182 (1999)
Update date:2022-08-16
Topics:
Uchiro, Hiromi
Kobayashi, Susumu
A new and efficient method for the non-aqueous reduction of sulfonyl chlorides to affored the corresponding thiols by use of a dichlorodimethylsilane-zinc-dimethylacetamide system was successfully developed. Various aromatic thiols were prepared in high yield by easy operation. Continuous reactions with the above reduction using the prepared thiol were also demonstrated.
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