Tetrahedron Letters p. 7483 - 7486 (1997)
Update date:2022-08-29
Topics:
Haley, Michael M.
Bell, Michael L.
Brand, Stephen C.
Kimball, David B.
Pak, Joshua J.
Wan, W. Brad
Addition of K2CO3 to standard Eglinton coupling conditions effects a one-pot desilylation/dimerization reaction of alkynyltrimethylsilanes. Use of this procedure on substituted phenylbutadiynylsilanes ultimately leads to the formation of dehydrobenzoannulenes possessing an unprecedented number of acetylene linkers.
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