Journal of Organometallic Chemistry p. 57 - 62 (1991)
Update date:2022-08-11
Topics:
Andriamizaka, Jean-Dominique
Couret, Claude
Escudie, Jean
Laporterie, Andre
Manuel, Georges
Regitz, Manfred
The (6-7,8-9)-dibenzo-2,3-dimethyl-5-germa <4,4>-spironona-1,3-diene 6, the first representative of a new type of germole, has been synthesized.This spirogermole reacts with maleic anhydride and t-butylphosphaacetylene by <2 + 4> cycloadditions, which involve exclusively the 2,3-dimethylgermole moiety.The adduct 9 obtained with the phosphaalkyne undergoes a thermal decomposition leading to the corresponding phosphabenzene.
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