Journal of Organic Chemistry p. 2165 - 2169 (1989)
Update date:2022-08-17
Topics:
Lu, F. L.
Keshavarz-K., M.
Srdanov, G.
Jacobson, R. H.
Wudl, F.
A "one-pot" preparation of the title 1,2-dithiole-3-thiones as well as the preparation and characterization of methyl 5-(methylthio)-2-thioxo-1,3-dithiole-4-dithiocarboxylate (3) are described.The X-ray structure determination of an iodine complex of the dithiolodithiole 5 is described in detail.The structure shows that this is a molecular solid with unusual three-dimensional intermolecular sulfur-sulfur "bonding".
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Doi:10.1002/cber.19701030328
(1970)Doi:10.1039/jr9400001134
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(2012)
