Synthetic Communications p. 3435 - 3438 (1999)
Update date:2022-08-11
Topics:
Wang, Cai-Lan
Wang, Xiao-Xia
Wang, Xiao-Yang
Xiao, Jun-Ping
Wang, Yu-Lu
A convenient method using FeCl3 as oxidant to dehydrogenate symmetric hydrazo compounds is reported for the first time. The method is superior to other known methods for dehydrogenating ArNHNHAr . It needs only cheap and less toxic reagents, mild conditions and short reaction time. Eight symmetric azo compounds are prepared in good yields.
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