Tetrahedron Letters p. 6031 - 6032 (1988)
Update date:2022-08-11
Topics:
O'Bannon, P. E.
Carroll, Patrick J.
Dailey, William P.
Nitrodiazoacetic acid was prepared and its structure determined by low temperature X-ray crystallography.There is good agreement between the experimentally determined structure and that calculated at the ab initio rhf/3-21G level of theory.The acid is stable in neat trifluoroacetic acid and less stable in neutral non-polar solutions.In neutral polar solutions it undergoes rapid decarboxylation to yield nitrodiazomethane.
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