
Synthesis p. 367 - 368 (1992)
Update date:2022-08-24
Topics:
Gajda
Matusiak
Diethyl 1-azidoalkylphosphonates were obtained in high yield, and under mild conditions by the reaction of diethyl 1-hydroxyalkylphosphonates with hydrazoic acid in the presence of triphenylphosphine/diethyl azodicarboxylate (the Mitsunobu reaction).
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