Journal of the Chemical Society. Chemical communications p. 830 - 832 (1992)
Update date:2022-08-12
Topics:
Barker, James
Cook, Stephen L.
Lasterra-Sanches M. Elena
Thomas, Susan E.
Addition of methyllithium followed by tertiary haloalkanes to readily available and air-stable (methyl 2-acetamidoacrylate)tricarbonyliron(0) 1, gives protected β,β,β-trialkyl α-amino acids which are hydrolysed to give tert-leucine 10 and the new α-amino acids 2-amino-3,3-dimethylpentanoic acid 11 and 2-amino-3,3-dimethylhexanoic acid 12.
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