Tetrahedron Letters p. 1765 - 1768 (1993)
Update date:2022-08-02
Topics:
Martin, Thomas J.
Schmidt, Richard R.
Reaction of sialyl phosphites 1 and 2 with dibenzyl phosphate and phenyl phosphate furnished without addition of a catalyst directly the corresponding sialyl phosphates 3 and 4, respectively, in good yields. Similarly, reaction of 1 with acetylated CMP 5 afforded exclusively β-configurated acetylated CMP-Neu-5-Ac (6); which was readily transformed into natural sialyl donor CMP-Neu-5-Ac (7).
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