A procedure for the large scale preparation of N(ε)-Alloc-lysine and N(ε)-Alloc-N(α)-Fmoc-lysine

Article abstract of DOI:10.1080/00397919308020400

This report describes a convenient procedure for a 100 g scale preparation of Fmoc-Lys(Alloc) in 85% yield. This method can be easily adapted to a near one-pot procedure with slightly reduced yields. Without requiring the isolation of the intermediate Lys(Alloc).

Full text of DOI:10.1080/00397919308020400

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Synthetic Communications: An
International Journal for Rapid
Communication of Synthetic
Organic Chemistry
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A Procedure for the Large
Scale Preparation of Nε-Alloc-
lysine and Nε-Alloc-Nα-Fmoc-
lysine
Anna Crivici a & Gilles Lajoie a
a Guelph-Waterloo Centre for Graduate Work in
Chemistry, Department of Chemistry , University of
Waterloo , Waterloo, Ontario, Canada , N2L 3G1
Published online: 24 Sep 2006.
To cite this article: Anna Crivici & Gilles Lajoie (1993) A Procedure for the Large
Scale Preparation of Nε-Alloc-lysine and Nε-Alloc-Nα-Fmoc-lysine, Synthetic
Communications: An International Journal for Rapid Communication of Synthetic
Organic Chemistry, 23:1, 49-53, DOI: 10.1080/00397919308020400
To link to this article: http://dx.doi.org/10.1080/00397919308020400
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