Molecules p. 523 - 527 (2006)
Update date:2022-08-17
Topics:
Prakash, Om
Pannu, Kamaljeet
Prakash, Richa
Batra, Anita
Reaction of various ketones with [hydroxy(tosyloxy)iodo]benzene (HTIB) followed by treatment of the α-tosyloxy ketones thus generated in situ with NaN3 offers a one-pot procedure for the synthesis of α-azido ketones. The HTIB used in this conversion may also be generated in situ by using iodosobenzene in combination with p-toluene-sulphonic acid.
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