A Novel Stereoselective Synthesis of (Z)-3-Iodo-3-alken-1-one from 2-Alkyn-1-one

DOI: 10.1016/S0040-4039(00)77168-1

Source and publish data:

Tetrahedron Letters p. 2553 - 2554 (1994)

Update date:2022-08-29

Topics:

Authors:

Luo, Fen-Tair

Kumar, K. Ajay

Hsieh, Li-Chen

Wang, Ren-Tzong

Read Full Text PDF DownLoad Join now for total 90,000,000 free articles

Article abstract of DOI:10.1016/S0040-4039(00)77168-1

A one-pot reaction of 2-alkyn-1-one with sodium iodide/acetonitrile/trimethylsilyl chloride/water or trimethylsilyl iodide/acetonitrile at 25 deg C gave almost exclusively (Z)-3-iodo-3-alken-1-one in good yields.

Full text of DOI:10.1016/S0040-4039(00)77168-1

Products guided by the article

Product name:(3Z)-3-iodo-1-phenylnon-3-en-1-one

Cas No:155797-06-1

R&D Labs maybe for 155797-06-1

Sanming Coffer Fine Chemical Industrial Co., Ltd

website:http://www.cofferxm.com/

Contact:+86-598-5853979

Address:Jin-sha Yuan Chuang-ye Park,Hi-Tech Development Zone,Sanming City P.R.China
JIAXING SUNS INTERNATIONAL TRADE CO LTD

Contact:18367306858

Address:No.123,Huixin Avenue,Huimin Dist
WUXI HONOR SHINE CHEMICAL CO.,LTD

Contact:+86-510-83593312

Address:No.1699 Huishan avenue,Huishan district,Wuxi ,Jiangsu,China,214177.(Wuxi Huishan Ecomonic Develop Zone )
Jiande City Silibase Silicone New Material Manufacture Co., Ltd.

Contact:15967177856

Address:Genglou Industrial Development Area
Changzhou Medi-tech Bioscientific Co., Ltd.(expird)

Contact:86-519-83246372

Address:Number 115 Menghedadao Road, Changzhou, Jiangsu, China

Relevant to this article

Acid-Base Properties of Highly Substituted Diaminonaphtalenes

Doi:10.1039/P29870000243
(1987)
Synthesis of 1,1-Diborylalkenes through a Br?nsted Base Catalyzed Reaction between Terminal Alkynes and Bis(pinacolato)diboron

Doi:10.1002/anie.201509218
(2015)
A permanently porous single molecule H-bonded organic framework for selective CO₂ capture

Doi:10.1039/c6cc02964g
(2016)
An NMR, IR and theoretical investigation of the methyl effect on conformational isomerism in 3-fluoro-3-methyl-2-butanone and 1-fluoro-3,3-dimethyl-2-butanone

Doi:10.1002/poc.471
(2002)
Cyclic enolates of Ni and Pd: Equilibrium between C- and O-bound tautomers and reactivity studies

Doi:10.1002/chem.200500622
(2005)
One step preparation of bromo-2-pyrones via bromo-decarboxylation of 2-pyrone-carboxylic acids

Doi:10.1016/S0040-4039(00)02182-1
(2001)

Article Doi