A Novel Stereoselective Synthesis of (Z)-3-Iodo-3-alken-1-one from 2-Alkyn-1-one

DOI: 10.1016/S0040-4039(00)77168-1

Source and publish data:

Tetrahedron Letters p. 2553 - 2554 (1994)

Update date:2022-08-29

Topics:

Authors:

Luo, Fen-Tair

Kumar, K. Ajay

Hsieh, Li-Chen

Wang, Ren-Tzong

Read Full Text PDF DownLoad Join now for total 90,000,000 free articles

Article abstract of DOI:10.1016/S0040-4039(00)77168-1

A one-pot reaction of 2-alkyn-1-one with sodium iodide/acetonitrile/trimethylsilyl chloride/water or trimethylsilyl iodide/acetonitrile at 25 deg C gave almost exclusively (Z)-3-iodo-3-alken-1-one in good yields.

Full text of DOI:10.1016/S0040-4039(00)77168-1

Products guided by the article

Product name:(3Z)-3-iodo-1-phenylnon-3-en-1-one

Cas No:155797-06-1

R&D Labs maybe for 155797-06-1

Beijing eternalchem Co,. Ltd

Contact:+86-10-59484199

Address:No.58-A1026 Liangguan Street
Lian Xing Chemical Co.,Ltd.

Contact:0792-8228321

Address:10TH Floor No.121 binjiang Road Xunyang District
xuri chemicals co., ltd

Contact:86-516-66656369

Address:The west road of Huaihai, Xuzhou, China
NEWSTAR CHEM ENTERPRISE LTD.

Contact:0572-2722882

Address:1201,F3,xinghuibandao,
Siwei Development Group Ltd.

website:http://www.chinapharmas.com

Contact:86-571-82881840

Address:Rm2-2-503 Zhongdingyuan, Xianghurenjia Wenyan Xiaoshan, Hangzhou China

Relevant to this article

Acid-Base Properties of Highly Substituted Diaminonaphtalenes

Doi:10.1039/P29870000243
(1987)
Synthesis of 1,1-Diborylalkenes through a Br?nsted Base Catalyzed Reaction between Terminal Alkynes and Bis(pinacolato)diboron

Doi:10.1002/anie.201509218
(2015)
A permanently porous single molecule H-bonded organic framework for selective CO₂ capture

Doi:10.1039/c6cc02964g
(2016)
An NMR, IR and theoretical investigation of the methyl effect on conformational isomerism in 3-fluoro-3-methyl-2-butanone and 1-fluoro-3,3-dimethyl-2-butanone

Doi:10.1002/poc.471
(2002)
Cyclic enolates of Ni and Pd: Equilibrium between C- and O-bound tautomers and reactivity studies

Doi:10.1002/chem.200500622
(2005)
One step preparation of bromo-2-pyrones via bromo-decarboxylation of 2-pyrone-carboxylic acids

Doi:10.1016/S0040-4039(00)02182-1
(2001)

Article Doi