Synthesis p. 1219 - 1220 (1992)
Update date:2022-08-11
Topics:
Lin
Ku
Shiao
A new method was developed for converting nitriles into primary thioamides. Treatment of various nitriles 1 with 1.5-2.5 equivalents of sodium trimethylsilyl sulfide (sodium trimethylsilanethiolate) in 1,3-dimethyl-2-imidazolidinone at 20-35°C for 4-30 hours gave the corresponding thioamides 2 in 27-80% yield.
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Doi:10.1021/jp047623+
(2004)Doi:10.1039/a708977e
(1998)Doi:10.1039/c3lc41398e
(2013)Doi:10.1021/ja0612403
(2006)Doi:10.1055/s-0037-1610671
(2018)Doi:10.1039/d0cc01238f
(2020)
