Tetrahedron Letters p. 4189 - 4192 (1995)
Update date:2022-08-17
Topics:
Bradford, Cara L.
Fleming, Steven A.
Ward, Susan C.
Substituted cyclobutenes were synthesized by irradiation of silicon tethered ene-ynes.Irradiation of a silicon tethered bisphenylalkyne resulted in cycloaddition and rearrangement to a substituted naphthalene.A diradical intermediate which resembles known DNA cleaving molecules is proposed. - Key Words: 2+2 photocycloaddition, alkoxysilane photochemistry, cyclobutene synthesis
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