Identification of the positional isomers of 2-fluorobenzoic acid 1-O-acyl glucuronide by directly coupled HPLC-NMR

DOI: 10.1021/ac00115a006

Source and publish data:

Analytical Chemistry p. 3401 - 3404 (1995)

Update date:2022-08-29

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Authors:

Sidelmann, Ulla G.

Gavaghan, Claire

Carless, Howard A. J.

Farrant, R. Duncan

Lindon, John C.

Wilson, Ian D.

Nicholson, Jeremy K.

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Article abstract of DOI:10.1021/ac00115a006

Directly coupled HPLC-¹H NMR was used in the "stop-flow" mode to separate and rapidly identify an equilibrated mixture of ester glucuronide isomers formed spontaneously by intramolecular rearrangement reactions (internal acyl migration and muta

Full text of DOI:10.1021/ac00115a006

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