Phosphorus, Sulfur and Silicon and the Related Elements p. 239 - 249 (2000)
Update date:2022-08-17
Topics:
Tazaki, Masato
Okada, Kenji
Yakata, Kenshi
Nakano, Koji
Sakai, Masashi
Yonemitsu, Tadashi
High purity synthesis of ω-ferrocenylalkanethiols (Fc(CH2)n-SH, n=6, 8, 11) was developed for their use in self-assembled monolayers on gold surface. The method employs a separation and purification of isothiuronium salt 6 to improve the purity of final products 7. The use of hazardous mercury in the Clemmensen reduction of acylferrocene 4 to alkylferrocenes 5 is avoided by an alternative LAH/AlCl3 reduction.
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