Journal of Organometallic Chemistry p. 143 - 148 (1986)
Update date:2022-08-16
Topics:
Birkofer, Leonhard
Grafen, Klaus
By hydrosilation of triethoxyvinylsilane (1), 1,5-hexadiene (10) and 3,3-dimethyl-3-sila-1,4-pentadiene (14) with triethoxysilane (2) we obtained 1,2-bis(triethoxysilyl)ethane (3), 1,6-bis(triethoxysilyl)hexane (11) and 1,5-bis(triethoxysilyl)-3,3-dimethyl-3-silapentane (15).The reaction of 3 with triethanolamine (4), triisopropanolamine (6) and tris(1-t-butyl-ethanol)amine (8) leads to the 1,2-disilatranylethanes 5, 7 and 9.The 1,6-disilatranylhexanes 12 and 13 are formed from 11, 4 and 6 respectively, and 15 with 4 gives 3,3-dimethyl-1,5-disilatranyl-3-silapentane (16).
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