Fast Synthesis of Amino Acid Salts and Lactams without Solvent under Microwave Irradiation

DOI: 10.1039/c39950001101

Source and publish data:

Journal of the Chemical Society. Chemical communications p. 1101 - 1102 (1995)

Update date:2022-09-26

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Authors:

Laurent, Alain

Jacquault, Patrick

Martino, Jean-Louis Di

Hamelin, Jack

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Article abstract of DOI:10.1039/c39950001101

Hydroxylamine-O-sulfonic acid reacts with alicyclic ketones over SiO2 under microwave irradiation to give an amino acid salt, which cyclises in high yield to the corresponding lactam after work up in basic medium.

Full text of DOI:10.1039/c39950001101

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