Fast Synthesis of Amino Acid Salts and Lactams without Solvent under Microwave Irradiation

DOI: 10.1039/c39950001101

Source and publish data:

Journal of the Chemical Society. Chemical communications p. 1101 - 1102 (1995)

Update date:2022-09-26

Topics:

Authors:

Laurent, Alain

Jacquault, Patrick

Martino, Jean-Louis Di

Hamelin, Jack

Read Full Text PDF DownLoad Join now for total 90,000,000 free articles

Article abstract of DOI:10.1039/c39950001101

Hydroxylamine-O-sulfonic acid reacts with alicyclic ketones over SiO2 under microwave irradiation to give an amino acid salt, which cyclises in high yield to the corresponding lactam after work up in basic medium.

Full text of DOI:10.1039/c39950001101

View Article Online / Journal Homepage / Table of Contents for this issue

Products guided by the article

Product name:Cyclohexanonoxim-hydrogensulfat

Cas No:19721-16-5

R&D Labs maybe for 19721-16-5

Shanghai Bojing Chemical Co., Ltd.

Contact:021-37122233

Address:6F Buildiing 11,No.388,Baifu Road,District Fengxian.Shanghai, China.
SHIFANG SUHONG CHEMICAL CO.,LTD

Contact:+86-838-2224563

Address:Room 1207 Zongchen Sunshine No.128 Taishan South Road,Deyang City,Sichuan China
Jiangxi Biochem Co.,Ltd

Contact:86-791-86629460

Address:1-6F, 118 Xinzhou road, Nanchang, Jiangxi, China
zhangjiagang bonded areas banggao co;ltd

website:http://www.shunchangchem.com

Contact:0086-13921972933

Address:Dongsha Chemical Zone.Zhangjiagang, Jiangsu Province
LIDE PHARMACEUTICALS LIMITED

website:http://www.lidepharma.com

Contact:+86-25-58409506

Address:Chungking Express Nos.36 Nathan Road，Kowloon, HK

Relevant to this article

Nonplanar Butterfly-Shaped π-Expanded Pyrrolopyrroles

Doi:10.1002/chem.201603282
(2016)
Preparation, antimicrobial evaluation, and mutagenicity of [2- hydroxyaryl]-[1-methyl-5-nitro-1H-2-imidazolyl]methanols, [5-tert-butyl-2- methylaminophenyl]-[1-methyl-5-nitro-1H-2-imidazolyl] methanol, and [2- hydroxyaryl]-[1-methyl-5-nitro-1H-2-imidazolyl] ketones

Doi:10.1016/S0968-0896(97)00138-7
(1997)
Doi:10.1021/ja01244a023
(1943)
Synthesis of the benzo[b]fluorene core of the kinamycins by arylalkyne-allene and arylalkyne-alkyne cycloadditions

Doi:10.1002/ejoc.200500926
(2006)
New findings on the hemetsberger-knittel reaction (synthetic studies on indoles and related compounds. XLIII(1))

Doi:10.1248/cpb.45.1739
(1997)
Highly regioselective ring opening of epoxides with polymer supported phenoxide and naphthoxide anions

Doi:10.1081/SCC-200026220
(2004)

Article Doi