Tetrahedron Letters p. 491 - 494 (1984)
Update date:2022-08-11
Topics:
Corey, E. J.
Gross, Andrew W.
Di-t-alkylamines can be synthesized efficiently by a three-step process: (1) oxidation of a t-alkylamine to a t-alkylnitroso compound with peracetic acid in ethyl acetate (2) conversion of the t-alkylnitroso compound to a tri-t-alkylhydroxylamine by successive trapping of two t-butyl radicals and (3) sodium naphthalide reduction to the di-t-alkylamine.
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