Tetrahedron p. 6645 - 6658 (1990)
Update date:2022-08-17
Topics:
Biller, Scott A.
Forster, Cornelia
A synthetic route to isoprenoid (phosphinylmethyl)phosphonates (PMPs), stable analogues of the biologically important diphosphates, is described.This method involves the reaction of an α-phosphonate carbanion with an isoprenoid phosphonochloridate to provide the PMP triesters, followed by ester cleavage with TMSBr or TMSI. 13C NMR, 31P NMR, 19F NMR and FAB-MS data were employed for the characterization of PMP salts and triesters.
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Doi:10.1002/chem.202002030
(2020)Doi:10.1021/ic100586h
(2010)Doi:10.1007/s11164-016-2750-1
(2017)Doi:10.1021/jp012709d
(2001)Doi:10.1007/BF01552758
(1932)Doi:10.1007/BF00988805
(1976)
