175. Synthesis of a Fullarene Derivative of Benzocrown-6 by Diels-Alder Reaction: Complexation Ability, Amphiphilic Properties, and X-Ray Crystal Structure of Dimethoxy-1,9-(methanobenzenomethano)fullerene Benzene Clathrate

DOI: 10.1002/hlca.19930760704

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Helvetica Chimica Acta p. 2445 - 2453 (1993)

Update date:2022-08-11

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Authors:

Diederich, Francois

Jonas, Ulrich

Gramlich, Volker

Herrmann, Andreas

Ringsdorf, Helmut

Thilgen, Carlo

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Article abstract of DOI:10.1002/hlca.19930760704

A fullerene derivative 1 of benzo<18>crown-6 was obtained by Diels-Alder addition of fullerene<60> (C60) to the ortho-quinodimethane prepared in situ from 4,5-bis(bromomethyl)benzo<18>crown-6 (3) with Bu4NI in toluene.Extraction experiments show that the

Full text of DOI:10.1002/hlca.19930760704

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