gem-Difluorination of 1,3-dithiolanes with the hexafluoropropene-diethylamine reagent and N-iodosuccinimide or 1,3-dibromo-5,5-dimethylhydantoin

DOI: 10.1016/0022-1139(94)03187-5

Source and publish data:

Journal of Fluorine Chemistry p. 9 - 12 (1995)

Update date:2022-08-16

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Authors:

Shimizu, Makoto

Maeda, Takashi

Fujisawa, Tamotsu

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Article abstract of DOI:10.1016/0022-1139(94)03187-5

gem-Difluoro compounds are readily prepared from 1,3-dithiolanes in good yield on treatment with hexafluoropropene-diethylamine/1,3-dibromo-5,5-dimethylhydantoin or /N-iodosuccinimide/water. - Keywords: gem-Difluorination; 1,3-Dithiolanes; NMR spectroscop

Full text of DOI:10.1016/0022-1139(94)03187-5

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