Canadian Journal of Chemistry p. 673 - 675 (1982)
Update date:2022-08-10
Topics:
Armstrong, Rosemary J.
Harris, Francis L.
Weiler, Larry
The allylsilanes 5 (a, R=(CH3)2CCHCH2; b, R=(CH3)2CCHCH2CH2C(CH3)CHCH2) were prepared by a nickel(II) catalyzed coupling of trimethylsilylmethylmagnesium chloride with the enol phosphate of the corresponding β-keto esters.Stannic chloride and mercuric trifluoroacetate effected a cyclization of 5.The product from 5b was converted into the marine natural product, albicanyl acetate (1).
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(1982)
