Synthesis p. 948 - 949 (1985)
Update date:2022-08-29
Topics:
Brandsma, L.
Jong, R. L. P. de
VerKruijsse, H. D.
The cyclocondensation of methyl dithiocarbamate with chloroacetaldehyde in aqueous ethanol affords 2-methylthio-1,3-thiazole (82-88percent) which is demethylsulfenylated to 1,3-thiazole (78-81percent) by reaction with lithium in liquid ammonia followed by hydrolysis with aqueous ammonia chloride.
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Doi:10.1002/j.2162-6057.2002.tb01057.x
(1931)Doi:10.1016/j.bmc.2015.06.055
(2015)Doi:10.1016/S0040-4039(00)87331-1
(1982)Doi:10.1021/ja00387a063
(1982)Doi:10.1016/S0040-4020(97)00654-6
(1997)Doi:10.1021/j100370a080
(1990)
