HMDS-promoted in situ amidation reactions of carboxylic acids and amines

DOI: 10.1016/S0040-4039(99)00505-5

Source and publish data:

Tetrahedron Letters p. 3419 - 3422 (1999)

Update date:2022-08-11

Topics:

Authors:

Chou, Wen-Chih

Chou, Ming-Chen

Lu, Yann-Yu

Chen, Shyh-Fong

Read Full Text PDF DownLoad Join now for total 90,000,000 free articles

Article abstract of DOI:10.1016/S0040-4039(99)00505-5

A number of N-acylalkylenediamines were synthesized in high yields by in situ monoamidation of carboxylic acids with diamines. The amidation reactions were carried out simply by heating the substrates at 110 °C for 5-24 h in the presence of HMDS.

Full text of DOI:10.1016/S0040-4039(99)00505-5

Products guided by the article

Product name:NSC 351869

Cas No:31350-27-3

R&D Labs maybe for 31350-27-3

Shanghai Massive Chemical Technology Co., Ltd.

website:http://www.massivechem.com/

Contact:+86 21 34943721

Address:Room 435, 4th floor, Building 9, No. 2568 Gudai Road,Minhang District, Shanghai,
Winchem Industrial Co. Ltd.(expird)

Contact:86-574-83851061 86-574-87083208

Address:Room 905, No.3 Building,East Business Center, 456 Xingning Road, Ningbo City,China
Li's chemicals

Contact:+86-15850770348

Address:51 OF XIANGFANGCUN ROAD, Nanjing 210002, China
Cerametek Materials（ShenZhen）Co., Ltd.

Contact:+86-755-2324.2554

Address:A3-#9, YongChuan Street, Suite 501
Dongying J&M Chemical Co., Ltd,

Contact:546-8551108

Address:Room 1219, Zisheng Mansion, Zibo Road, Dongying, Shandong, China

Relevant to this article

Doi:10.1021/jo00908a025
(1975)
Syntheses, structures and electrochemical properties of ruthenium(II/III) complexes with tetradentate Schiff base ligands

Doi:10.1080/00958972.2019.1566541
(2019)
18F fluorination of a RGD peptide under ambient aqueous conditions">A localized tolerance in the substrate specificity of the fluorinase enzyme enables "last-step" ¹⁸F fluorination of a RGD peptide under ambient aqueous conditions

Doi:10.1002/anie.201403345
(2014)
Excited-state acidity of bifunctional compounds: Part 5 5-(2-hydroxyphenyl)-3-phenyl-1,2,4-oxadiazole and 3-(2-hydroxyphenyl)-5-phenyl-1,2,4-oxadiazole

Doi:10.1039/a702708g
(1997)
Phage-Guided Targeting, Discriminative Imaging, and Synergistic Killing of Bacteria by AIE Bioconjugates

Doi:10.1021/jacs.9b12936
(2020)
Synthesis and trazodone-like pharmacological profile of 1- and 2-<3-<4-(X)-1-piperazinyl>-propyl>benzotriazoles

Doi:10.1016/0223-5234(93)90053-H
(1993)

Article Doi