HMDS-promoted in situ amidation reactions of carboxylic acids and amines

DOI: 10.1016/S0040-4039(99)00505-5

Source and publish data:

Tetrahedron Letters p. 3419 - 3422 (1999)

Update date:2022-08-11

Topics:

Authors:

Chou, Wen-Chih

Chou, Ming-Chen

Lu, Yann-Yu

Chen, Shyh-Fong

Read Full Text PDF DownLoad Join now for total 90,000,000 free articles

Article abstract of DOI:10.1016/S0040-4039(99)00505-5

A number of N-acylalkylenediamines were synthesized in high yields by in situ monoamidation of carboxylic acids with diamines. The amidation reactions were carried out simply by heating the substrates at 110 °C for 5-24 h in the presence of HMDS.

Full text of DOI:10.1016/S0040-4039(99)00505-5

Products guided by the article

Product name:NSC 351869

Cas No:31350-27-3

R&D Labs maybe for 31350-27-3

Nanjing Fayekong Chemcial Co.,Ltd(expird)

Contact:86-25-58813444

Address:Rm 1503, Unit 1, Building 5, Zijinnanyuan, Nanjing, Jiangsu, China
Ceresking Ecology & Technology co.,ltd

Contact:86 22 66218397

Address:Room 1613, Zheshang Mansion, No. 1988, Yingbin Avenue, Binhai New District, Tianjin,China.
Changzhou Foreign Trade Corp

Contact:+86-519-86623222

Address:29F/D, 99 Yanling West Road, Changzhou, Jiangsu, China
Changzhou Kingyo Chemical Corporation Ltd.

website:http://www.kingyochem.com

Contact:+86-519-85105717

Address:19# Wuqing North Road, Changzhou , Jiangsu, China
Synchem Pharma Co.,Ltd(expird)

Contact:+0086-21-61984905-1

Address:Building 60,Zimian Park, LongYang industrial Area, 1515Nong，Yuandong Road Fengxian District, Shanghai ,China

Relevant to this article

Doi:10.1021/jo00908a025
(1975)
Syntheses, structures and electrochemical properties of ruthenium(II/III) complexes with tetradentate Schiff base ligands

Doi:10.1080/00958972.2019.1566541
(2019)
18F fluorination of a RGD peptide under ambient aqueous conditions">A localized tolerance in the substrate specificity of the fluorinase enzyme enables "last-step" ¹⁸F fluorination of a RGD peptide under ambient aqueous conditions

Doi:10.1002/anie.201403345
(2014)
Excited-state acidity of bifunctional compounds: Part 5 5-(2-hydroxyphenyl)-3-phenyl-1,2,4-oxadiazole and 3-(2-hydroxyphenyl)-5-phenyl-1,2,4-oxadiazole

Doi:10.1039/a702708g
(1997)
Phage-Guided Targeting, Discriminative Imaging, and Synergistic Killing of Bacteria by AIE Bioconjugates

Doi:10.1021/jacs.9b12936
(2020)
Synthesis and trazodone-like pharmacological profile of 1- and 2-<3-<4-(X)-1-piperazinyl>-propyl>benzotriazoles

Doi:10.1016/0223-5234(93)90053-H
(1993)

Article Doi