HMDS-promoted in situ amidation reactions of carboxylic acids and amines

DOI: 10.1016/S0040-4039(99)00505-5

Source and publish data:

Tetrahedron Letters p. 3419 - 3422 (1999)

Update date:2022-08-11

Topics:

Authors:

Chou, Wen-Chih

Chou, Ming-Chen

Lu, Yann-Yu

Chen, Shyh-Fong

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Article abstract of DOI:10.1016/S0040-4039(99)00505-5

A number of N-acylalkylenediamines were synthesized in high yields by in situ monoamidation of carboxylic acids with diamines. The amidation reactions were carried out simply by heating the substrates at 110 °C for 5-24 h in the presence of HMDS.

Full text of DOI:10.1016/S0040-4039(99)00505-5

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