A convenient method for the transformation of alcohols into alkyl trifluoromethyl sulfides

DOI: 10.1055/s-1994-25422

Source and publish data:

Synthesis p. 145 - 146 (1994)

Update date:2022-08-16

Topics:

Authors:

Kolomeitsev

Chabanenko

Roschenthaler

Yagupolskii

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Article abstract of DOI:10.1055/s-1994-25422

Alkyl trifluoromethyl sulfides are prepared by phosphitylation of alcohols or α-hydroxy esters using bis(diethylamido)chlorophosphite followed by the reaction with bis(trifluoromethyl) disulfide under extremely mild conditions in near by quantitative yields.

Full text of DOI:10.1055/s-1994-25422

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