BEITRAEGE ZUR CHEMIE DER SCHEFELHALOGENIDE 15. DICHLOR-FLUOR-TRIFLUOROMETHYLSULFURAN, CF3SCl2F

DOI: 10.1016/S0022-1139(00)85020-4

Source and publish data:

Journal of Fluorine Chemistry p. 393 - 398 (1987)

Update date:2022-08-12

Topics:

Authors:

Minkwitz, Rolf

Nass, Ulrike

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Article abstract of DOI:10.1016/S0022-1139(00)85020-4

The preparation of the sulfurane CF3SCl2F is reported.Upon sublimation of the sulfonium salt CF3SCl2⁺AsF6^- the compounds CF3SCl2F and AsF5 coexist in the gaseous phase.After trapping AsF5 as KAsF6 extremely instable CF3SCl2F is isolated and characterised by IR-, Raman- and 19F-NMR-spectroscopy.

Full text of DOI:10.1016/S0022-1139(00)85020-4

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