Journal of Fluorine Chemistry p. 393 - 398 (1987)
Update date:2022-08-12
Topics:
Minkwitz, Rolf
Nass, Ulrike
The preparation of the sulfurane CF3SCl2F is reported.Upon sublimation of the sulfonium salt CF3SCl2+AsF6- the compounds CF3SCl2F and AsF5 coexist in the gaseous phase.After trapping AsF5 as KAsF6 extremely instable CF3SCl2F is isolated and characterised by IR-, Raman- and 19F-NMR-spectroscopy.
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(1988)
