Synthesis p. 893 - 894 (1988)
Update date:2022-08-25
Topics:
Raffaelli, Andrea
Rosini, Carlo
Dini, Massimo
Salvadori, Piero
Hydroformylation of acenaphthylene using di-μ-chlorotetracarbonyldirhodium/triphenylphosphine as catalytic precursor affords acenaphthene-1-carboxaldehyde under mild conditions in 80percent yield.This compound is easily transformed, via dehydration of the corresponding oxime followed by hydrolysis of the nitrile, into acenaphthene-1-carboxylic acid in an overall yield of ca. 50percent.
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(1984)
