Facile syntheses of tris(trifluoromethyl) phosphine and difluorotris(trifluoromethyl)phosphorane

DOI: 10.1016/0022-1139(96)03471-9

Source and publish data:

Journal of Fluorine Chemistry p. 103 - 104 (1996)

Update date:2022-08-11

Topics:

Authors:

Goerg, Michaela

Roeschenthalera, Gerd-Volker

Kolomeitsev, Alexander A.

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Article abstract of DOI:10.1016/0022-1139(96)03471-9

Tris(trifluorornethyl)phosphine is easily available in high yield using the three component system P(NEt)₂)₃/CF₃Br/(PhO)₃P in HMPA. Addition of chlorine and fluorination with zinc difluoride yield difluorotris(trifluoromethyl)phosphorane.

Full text of DOI:10.1016/0022-1139(96)03471-9

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