Journal of Fluorine Chemistry p. 103 - 104 (1996)
Update date:2022-08-11
Topics:
Goerg, Michaela
Roeschenthalera, Gerd-Volker
Kolomeitsev, Alexander A.
Tris(trifluorornethyl)phosphine is easily available in high yield using the three component system P(NEt)2)3/CF3Br/(PhO)3P in HMPA. Addition of chlorine and fluorination with zinc difluoride yield difluorotris(trifluoromethyl)phosphorane.
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